Hi all,
I would like some advice on what could be the issue when an Elan 6100 is consistently failing the Interference check B for method 6020 for Copper. I am new on this machine, and with this method, and I am trying to find out where I should check. My trainer tells me (swears up down, left and right) that it is the machine and not the solution, the question is where in the machine?
The calibration curve is good, every other analyte in the interference check solution is passing (200 ppb +/- 10%) and copper is just falling. Yesterday it barely failed at 156, today it is dropping to 145, and we need it to be at least 160 ppb. We have a new detector, the ICV/ICB is passing. It is passing the daily performance for everything, but the interference for copper is failing. And we need it so we can complete our IDL's for the 6020 method. My trainer keeps telling me it is the lens, but the lens has been cleaned, put back in, a different lens was cleaned and put back in, and it didn't change.
Any ideas on what might cause this to help a new person out on this machine?