Analysis of Lithium Complex

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PRAVEEN PALIWAL
PRAVEEN PALIWAL's picture
Analysis of Lithium Complex

Sir,

I want to analyze the LAEDA (Lithium Acetylide Ethylene Diamine complex) The cas No. is 6867-30-7. The sigma aldrich shows the assay against the titration with HCl. Iwant to know that how can we analyze this by titration. and what is the another procedure to analyze it. Can I analyze this on HPLC by the derivatization.
It is is water soluble so it is not possible to derivatized it by the benzoyl chloride (COCl), becasue before reacting with Lithium comples the acyl chloride reacts with the water.
So what is the procedure to analyze it???

Best regards

Praveen