Acetic Acid determination by Hplc conductivity detector

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saby2424
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Acetic Acid determination by Hplc conductivity detector

iam getting  big fluctuation in same vial injection area on conductivity detector . can any body tell me what sholud i try

Dr. Analytical
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Do you have any other methods

Do you have any other methods that use this detector?  If yes, then try those methods to see if the same problems are observed.

How big are the fluctuations?  What is the relative standard deviation?

What are the details for the equipment and method?

The problem could be either injector or detector.